• 文献标题:   Role of graphene in structural transformation of zirconium oxide
  • 文献类型:   Article
  • 作  者:   RANI S, KUMAR M, SHARMA S, KUMAR D
  • 作者关键词:   combustion synthesi, zro2, graphene oxide, xray diffraction, thermogravimetric analysi
  • 出版物名称:   JOURNAL OF SOLGEL SCIENCE TECHNOLOGY
  • ISSN:   0928-0707 EI 1573-4846
  • 通讯作者地址:   Kurukshetra Univ
  • 被引频次:   4
  • DOI:   10.1007/s10971-014-3401-x
  • 出版年:   2014

▎ 摘  要

Fine powders of zirconium oxide (ZrO2) were prepared using zirconium oxychloride by combustion method. The crystalline size of pure ZrO2 was in range of 14-45 nm. Graphene was incorporated in ZrO2 using graphene oxide as precursor and reducing it with hydrazine hydrate. X-Ray diffraction, Fourier transform infra-red spectroscopy, thermogravimetric analysis and Raman spectroscopy methods were used to characterize the samples. The role of graphene in structural transformation of ZrO2 to monoclinic phase was clearly observed.