• 文献标题:   Direct Optical Characterization of Graphene Growth and Domains on Growth Substrates
  • 文献类型:   Article
  • 作  者:   JIA CC, JIANG JL, GAN L, GUO XF
  • 作者关键词:  
  • 出版物名称:   SCIENTIFIC REPORTS
  • ISSN:   2045-2322
  • 通讯作者地址:   Peking Univ
  • 被引频次:   98
  • DOI:   10.1038/srep00707
  • 出版年:   2012

▎ 摘  要

We detailed a facile detection technique to optically characterize graphene growth and domains directly on growth substrates through a simple thermal annealing process. It was found that thermal annealing transformed the naked Cu to Cu oxides while keeping graphene and graphene-covered Cu intact. This increases the interference color contrast between Cu oxides and Cu, thus making graphene easily visible under an optical microscope. By using this simple method, we studied the factors that affect graphene nucleation and growth and achieved graphene domains with the domain size as large as similar to 100 mu m. The concept of chemically making graphene visible is universal, as demonstrated by the fact that a solution process based on selective H2O2 oxidation has been developed to achieve the similar results in a shorter time. These techniques should be valuable for studies towards elucidating the parameters that control the grains, boundaries, structures and properties of graphene.