• 文献标题:   One-pot sonochemical synthesis of CuS nanoplates decorated partially reduced graphene oxide for biosensing of dopamine neurotransmitter
  • 文献类型:   Article, Proceedings Paper
  • 作  者:   PALANISAMY S, VELMURUGAN S, YANG TCK
  • 作者关键词:   sonochemical synthesi, partially reduced graphene oxide, neurotransmitter, cus nanoplate, biosensor
  • 出版物名称:   ULTRASONICS SONOCHEMISTRY
  • ISSN:   1350-4177 EI 1873-2828
  • 通讯作者地址:   Natl Taipei Univ Technol
  • 被引频次:   4
  • DOI:   10.1016/j.ultsonch.2020.105043
  • 出版年:   2020

▎ 摘  要

The sonochemical methods have been used as a straight forward method for the synthesis of various composite materials, including the transition metal dichalcogenide composites. In the present work, we report a simple sonochemical synthesis of CuS nanoplates decorated partially reduced graphene oxide (PrGO) nanocomposite for the first time. The PrGO-CuS nanocomposite was synthesized using bath-sonication (frequency: 37 kHz; power: 150 W) of graphene oxide (GO), and CuS precursors at 80 degrees C for 60 min. The physicochemical characterization (FESEM, XRD, FTIR, and Raman spectroscopy) results confirmed the successful formation of CuS nanoplates on PrGO nanosheets. The as-synthesized PrGO-CuS nanocomposite was further utilized for electroanalysis of dopamine neurotransmitter. The obtained electroanalytical results revealed that PrGO-CuS nanocomposite has superior electrochemical activity towards dopamine than those obtained for GO, CuS, and GO-CuS composite. The fabricated biosensor shows a lower limit of detection (0.022 mu M) with a more comprehensive linear response range (0.1-155.1 mu M) for the detection of dopamine. Moreover, the PrGO-CuS nanocomposite electrode was successfully used for the detection of dopamine in bovine serum albumin.