▎ 摘　　要

Novel hierarchically porous and nitrogen, sulfur-codoped graphene-like microspheres (3D NS-GSs) are synthesized using Nimicrospheres as the template and using poly(vinylpyrrolidone) and (NH4)(2)S2O8 as the carbon and nitrogen precursor, respectively. As an anode material in lithium ion batteries, the 3D NS-GS electrode displays a superior capacity with excellent cycling stability.