▎ 摘　　要

Electrochemical regeneration suffers from low regeneration efficiency due to side reactions like oxygen evolution, as well as oxidation of the adsorbent. In this study, electrically conducting nanocomposites, including graphene/SnO2 (G/SnO2) and graphene/Sb-SnO2 (G/Sb-SnO2) were successfully synthesized and characterized using nitrogen adsorption, scanning electron microscopy, transmission electron microscopy, and Raman spectroscopy. Thereafter, the adsorption and electrochemical regeneration performance of the nanocomposites were tested using methylene blue as a model contaminant. Compared to bare graphene, the adsorption capacity of the new composites was 35 C mg(-1) for bare graphene. Consecutive loading and anodic electrochemical regeneration cycles of the nanocomposites were carried out in both NaCl and Na2SO4 electrolytes without loss of the nanocomposite, attaining high regeneration efficiencies (ca. 100%).