• 文献标题:   Synthesis of graphene oxide functionalized surface-imprinted polymer for the preconcentration of tetracycline antibiotics
  • 文献类型:   Article
  • 作  者:   LIU D, SONG NZ, FENG W, JIA Q
  • 作者关键词:  
  • 出版物名称:   RSC ADVANCES
  • ISSN:   2046-2069
  • 通讯作者地址:   Jilin Univ
  • 被引频次:   14
  • DOI:   10.1039/c5ra22462d
  • 出版年:   2016

▎ 摘  要

In this work, we synthesized graphene oxide functionalized a surface-imprinted polymer based on the self-polymerization of dopamine to generate the imprinted cavity. Using minocycline as the template molecule, effects of experimental conditions in the imprinting procedure such as g-MAPS@GO percentage, template concentration, and self-polymerization time of dopamine on the selectivity and performance of the prepared molecularly imprinted polymers were investigated. The characteristics of the prepared surface-imprinted polymer were determined by scanning electron microscope, transmission electron microscope, energy dispersive spectroscopy, Fourier-transformed infrared spectra, X-ray photoelectron spectroscopy, thermal gravimetric analysis, atomic force microscope, and water contact angle. The prepared graphene oxide functionalized surface-imprinted polymer showed good recognition capacity and enrichment performance for tetracycline antibiotics and was successfully applied to the detection of the target analytes in milk samples.