• 文献标题:   Low Temperature Reduction of Graphene Oxide Using Hot-plate for Nanocomposites Applications
  • 文献类型:   Article
  • 作  者:   HUSSEIN A, SARKAR S, KIM B
  • 作者关键词:   graphene, nanocomposite, mechanical propertie, fracture toughnes
  • 出版物名称:   JOURNAL OF MATERIALS SCIENCE TECHNOLOGY
  • ISSN:   1005-0302
  • 通讯作者地址:   Korea Univ Technol Educ
  • 被引频次:   7
  • DOI:   10.1016/j.jmst.2016.02.001
  • 出版年:   2016

▎ 摘  要

A green, easy to reproduce method to obtain thermally reduced graphene oxide (GO) is described. The only requirement is a heating source, like a hot plate, that can reach similar to 225 degrees C without any special setup requirements. Upon addition of graphene oxide, effective reduction could be achieved within 10 s. Starting flake size affects the yield of graphene, final structure and composition. A detailed characterization of the produced graphene using thermal analysis, spectroscopic methods, electron microscopy, X-ray diffraction and atomic force microscopy is presented. Application of the produced graphene as a filler to epoxy resin for mechanical reinforcement is also reported. Smaller flakes (D-50 = 5.7 mu m) showed improved ultimate tensile strength, fracture strain and plane strain fracture toughness compared to larger flakes (D-50 = 47.9 mu m) that showed negative effect. Both flake sizes showed a negligible effect on Young's modulus. Copyright (C) 2016, The editorial office of Journal of Materials Science & Technology. Published by Elsevier Limited. All rights reserved.