• 文献标题:   Structural and Optical Properties of Graphene Oxide Prepared by Modified Hummers' Method
  • 文献类型:   Article
  • 作  者:   SELVAKUMAR N, PRADHANL U, KRUPANIDHI SB, BARSHILIA HC
  • 作者关键词:   graphene oxide, graphite, modified hummers method, thermal annealing, optical propertie
  • 出版物名称:   CMCCOMPUTERS MATERIALS CONTINUA
  • ISSN:   1546-2218 EI 1546-2226
  • 通讯作者地址:   CSIR Natl Aerosp Labs
  • 被引频次:   2
  • DOI:  
  • 出版年:   2016

▎ 摘  要

Graphene oxide was synthesized from graphite flakes using modified Hummers' method. The interlayer spacings of graphite, graphite oxide and graphene oxide were measured using X-ray diffraction technique. The C/O atomic ratios of graphite oxide and graphene oxide were calculated from XPS measurements. The transformation of graphite to graphite oxide and finally to graphene oxide was clearly observed from the micro-Raman spectroscopy data and was confirmed from the FESEM micrographs. UV-VIS-NIR spectrophotometer was used to study the absorbance of graphene oxide and reduced graphene oxide samples. Finally, the chemically reduced graphene oxide was heat-treated in air to obtain chemically modified graphene.