• 文献标题:   Growth and characterization of graphene by chemical reduction of graphene oxide in solution
  • 文献类型:   Article
  • 作  者:   YAN J, ZHAO ZW, PAN LK
  • 作者关键词:   chemical reduction, graphene, thermal stability
  • 出版物名称:   PHYSICA STATUS SOLIDI AAPPLICATIONS MATERIALS SCIENCE
  • ISSN:   1862-6300 EI 1862-6319
  • 通讯作者地址:   Southeast Univ
  • 被引频次:   12
  • DOI:   10.1002/pssa.201084172
  • 出版年:   2011

▎ 摘  要

Graphene was synthesized by the modified Hummers method and a hydrazine reduction process. The obtained graphene was characterized by various diagnostic techniques, such as scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). A layer of transparency crumpled film was obtained with an interlayer spacing of 0.37 nm. The two typical peaks of 3415 and 1091 cm(-1) correlated to O-H and C-O were observed from the FTIR spectrum. The samples showed an enhanced thermal stability promoting the way for the research and the applications of graphene. (C) 2011 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim