• 文献标题:   One-step synthesis and characterization of reduced graphene oxide using chemical exfoliation method
  • 文献类型:   Article
  • 作  者:   GEBREEGZIABHER GG, ASEMAHEGNE AS, AYELE DW, DHAKSHNAMOORTHY M, KUMAR A
  • 作者关键词:   direct synthesi, reduction, oxidation, highefficient synthesi
  • 出版物名称:   MATERIALS TODAY CHEMISTRY
  • ISSN:   2468-5194
  • 通讯作者地址:   Mekelle Univ
  • 被引频次:   12
  • DOI:   10.1016/j.mtchem.2019.02.003
  • 出版年:   2019

▎ 摘  要

Graphene has many potential applications. Currently, its synthesis starts with the oxidation of graphite to graphene oxide followed by a separate reduction step. But, this leads to extra cost, prolonged time, and contamination. Here, we report the preparation of reduced graphene oxide (rGO) directly from graphite in a solution of potassium permanganate and concentrated sulfuric acid assisted by ultrasonication. The morphology, optical, chemical, thermal, microstructural, and electrical properties of prepared samples were studied using scanning transmission electron microscopy, selected area electron diffraction, ultra violet-visible spectroscopy, Fourier-transform infrared spectroscopy, thermogravimetric analysis, Raman spectroscopy, X-ray powder diffraction, and cyclic voltammeter, respectively. The analysis confirms that quality of rGO with thickness (similar to 0.36 nm) that can be dispersed in water with the desired properties was obtained. We can use this method to prepare rGO directly from graphite for energy storage. (C) 2019 Elsevier Ltd. All rights reserved.