▎ 摘　　要

This work reports a one-pot procedure of laser ablation on a graphite target in a liquid medium, based on the variation of different parameters such as target type, laser wavelength, and ablation medium, to obtain high-quality graphene nanosheets. The morphology of derived products was characterized by the field emission scanning electron microscopy (FE-SEM). Then, the morphology and structure of the optimized sample were characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD), ultraviolet-visible-near infrared (UV-vis-NIR) spectroscopy, Raman spectroscopy, and X-ray photoelectron spectroscopy (XPS). By controlling the laser ablation parameters, we were able to prepare micrometer-sized few-layer graphene nanosheets with mainly less than ten layers. Such synthesized graphene nanosheets were grown at the surface of a flexible graphite target, indicating many potential applications in fundamental research, electrochemical and as hydrophobic surfaces. (C) 2018 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.