• 文献标题:   Controlled synthesis of blue luminescent graphene quantum dots from carbonized citric acid: Assessment of methodology, stability, and fluorescence in an aqueous environment
  • 文献类型:   Article
  • 作  者:   MORE MP, LOHAR PH, PATIL AG, PATIL PO, DESHMUKH PK
  • 作者关键词:   graphene quantum dot, scientific microwave, blue luminescence, aqueous synthesi, carbonization
  • 出版物名称:   MATERIALS CHEMISTRY PHYSICS
  • ISSN:   0254-0584 EI 1879-3312
  • 通讯作者地址:   HR Patel Inst Pharmaceut Educ Res
  • 被引频次:   4
  • DOI:   10.1016/j.matchemphys.2018.08.046
  • 出版年:   2018

▎ 摘  要

The present investigation deals with a comparative assessment of various techniques for the synthesis of blue luminescence Graphene Quantum Dots (GQDs) using various equipments like furnace, domestic microwave synthesiser and scientific microwave synthesiser using citric acid as a precursor. A bottom-up method was adapted to develop photoluminescent (PL) GQDs and assessed for luminescence intensity of GQDs at different environmental conditions. The methodology requires very less concentration of NaOH to disperse GQDs. The present approach is advantageous over other conventional organic solvent mediated synthesis, as it requires less time, easy to reproduce and disperse in water, furthermore it produces stable fluorescence for a longer period of time at ambient temperature conditions. The synthesized GQDs are primarily characterized by UV for detection of the fluorescence intensity and simultaneously Ultraviolet-Visible (UV-Vis) spectroscopy and Fourier Transform Infra Red (FTIR) Spectroscopy to assess the up conversion from the precursor molecule. Apart from these techniques, Particle Size and Zeta Potential, Scanning Electron Microscopy (SEM), Elemental Analysis (EDX), Raman Spectroscopy and Fluorescence spectrophotometry were used to characterise synthesized GQDs.