• 文献标题:   Preparation and characterization of polyvinylpyrrolidone/cobalt ferrite functionalized chitosan graphene oxide (CoFe2O4@CS@GO-PVP) nanocomposite
  • 文献类型:   Article
  • 作  者:   MASOUMPARAST M, MOKHTARY M, KEFAYATI H
  • 作者关键词:   cofe2o4, graphene oxide, nanocomposite, polyvinylpyrrolidone, thermal stability
  • 出版物名称:   JOURNAL OF POLYMER ENGINEERING
  • ISSN:   0334-6447 EI 2191-0340
  • 通讯作者地址:   Islamic Azad Univ
  • 被引频次:   0
  • DOI:   10.1515/polyeng-2019-0331
  • 出版年:   2020

▎ 摘  要

Cobalt ferrite functionalized chitosan graphene oxide (CoFe2O4@CS@GO) was inserted successfully in polyvinylpyrrolidone (PVP), and its distribution was distinguished through scanning electron microscope (SEM) analysis. Furthermore, the thermal and structural characterizations of the CoFe2O4@CS@GO-PVP nanocomposite were accomplished via the TGA, DSC, FT-IR, and XRD methods. The magnetic characterization of the synthesized nanocomposite was specified by vibrating sample magnetometer (VSM). Results demonstrated the improved thermal stability of pure PVP with the addition of CoFe2O4@CS@GO. The DSC analysis results also showed that the glass transition temperature of 158.9 degrees C-164.8 degrees C was obtained for the CoFe2O4@CS@GO-PVP nanocomposites. The FT-IR spectra indicated that an interaction occurred between CoFe2O4@CS@GO and PVP. Due to a good distribution of CoFe2O4@CS@GO in the PVP matrix, the strong interaction shown by the similar to 18 cm(-1) red shift with good complexation of the carbonyl functional group of PVP with CoFe2O4@CS@GO was observed for the CoFe2O4 @CS@GO-PVP (5% w/w) nanocomposite.