• 文献标题:   Cadmium Ions Determination in Sea Food Samples Using Dipyridyl-Functionalized Graphene Nano-sheet
  • 文献类型:   Article
  • 作  者:   KARIMI M, ABOUFAZELI F, ZHAD HRLZ, SADEGHI O, NAJAFI E
  • 作者关键词:   modified graphene nanosheet, cd ii determination, solidphase extraction, faas, sea food
  • 出版物名称:   FOOD ANALYTICAL METHODS
  • ISSN:   1936-9751 EI 1936-976X
  • 通讯作者地址:   Islamic Azad Univ
  • 被引频次:   15
  • DOI:   10.1007/s12161-013-9671-z
  • 出版年:   2014

▎ 摘  要

In this work, graphene nano-sheets was modified by dipyridyl amine group and used as a novel sorbent for selective separation and preconcentration of cadmium ions. The sorbent was characterized by infrared spectroscopy, transmission electron microscopy, thermal analysis, and elemental analysis. The application of this sorbent was investigated in determination of cadmium ions in sea food samples by flame atomic absorption spectrometry. The effective parameters on adsorption and desorption of cadmium were optimized. The limit of detection, the relative standard deviation and the recovery of the established method were found to be 0.19 ng mL(-1), 1.6 %, and 99.1 %, respectively. The method was validated using various standard reference materials and was applied for cadmium determination in sea food sample.