• 文献标题:   A facile approach to prepare graphene via solvothermal reduction of graphite oxide
  • 文献类型:   Article
  • 作  者:   YUAN BH, BAO CL, QIAN XD, WEN PY, XING WY, SONG L, HU Y
  • 作者关键词:   nanostructure, chemical synthesi, atomic force microscopy, electron microscopy, thermogravimetric analysi
  • 出版物名称:   MATERIALS RESEARCH BULLETIN
  • ISSN:   0025-5408 EI 1873-4227
  • 通讯作者地址:   Univ Sci Technol China
  • 被引频次:   12
  • DOI:   10.1016/j.materresbull.2014.04.016
  • 出版年:   2014

▎ 摘  要

In this work, a facile reduction strategy is reported for the fabrication of graphene. Graphite oxide (GO) is reduced via a novel solvothermal reaction in a mixed solution of acetone and sodium hypochlorite (NaClO). The structure, surface chemistry, morphology and thermal stability of the as-prepared reduced graphene oxide (RGO) are characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, transmission electron microscopy (TEM), atomic force microscopy (AFM), thermogravimetric analysis (TGA) and X-ray photoelectron spectroscopy (XPS). The results indicate that most of the oxygenated groups in GO are effectively removed in this solvothermal reaction. The novel reduction method provides a simple, cost-effective and efficient strategy for the fabrication of graphene. Published by Elsevier Ltd.