• 文献标题:   Production and characterization of spark plasma sintered (Ti,Nb)B-2 solid solutions with graphene nanoplatelets and hexagonal boron nitride
  • 文献类型:   Article
  • 作  者:   AKARSU MK, AKIN I
  • 作者关键词:   boride, solid solution, gnp, hbn
  • 出版物名称:   CERAMICS INTERNATIONAL
  • ISSN:   0272-8842 EI 1873-3956
  • 通讯作者地址:  
  • 被引频次:   0
  • DOI:   10.1016/j.ceramint.2022.10.155 EA JAN 2023
  • 出版年:   2023

▎ 摘  要

For this study, (Ti,Nb)B-2 solid solutions were consolidated by spark plasma sintering. In addition, (Ti,Nb)B-2 with graphene nanoplatelets (GNPs) and hexagonal boron nitride (h-BN) were produced to evaluate the potential of the new structural materials. The phase formation, microstructure, mechanical properties, oxidation resistance and room temperature reflectance, and absorbance features of (Ti,Nb)B2 were investigated. X-ray diffraction and Transmission electron microscopy observations showed that a complete solid solution phase was formed when the samples were sintered at 1850 degrees C for 5 min under 50 MPa. Ti0.75Nb0.25B2 exhibited a relative density of similar to 98.6%, a hardness of similar to 20.5 GPa, and an indentation fracture toughness of similar to 3.4 MPa center dot m(1/2). It was found that the presence of 1 vol% h-BN as an additive enhanced the hardness (-10%) and fracture toughness (similar to 30%) of Ti0.75Nb0.25B2 by activating toughening mechanisms. The GNP added Ti0.75Nb0.25B2 proved to have better oxidation resistance and optical absorbance than the other materials used in the study.