• 文献标题:   A new analytical device incorporating a nitrogen doped lanthanum metal oxide with reduced graphene oxide sheets for paracetamol sensing
  • 文献类型:   Article
  • 作  者:   PONNAIAH SK, PRAKASH P, VELLAICHAMY B
  • 作者关键词:   nceo2 nanoparticle, reduced graphene oxide, electrochemical sensor, paracetamol
  • 出版物名称:   ULTRASONICS SONOCHEMISTRY
  • ISSN:   1350-4177 EI 1873-2828
  • 通讯作者地址:   Thiagarajar Coll
  • 被引频次:   15
  • DOI:   10.1016/j.ultsonch.2018.02.016
  • 出版年:   2018

▎ 摘  要

The novel N-CeO2 nanoparticles decorated on reduced graphene oxide (N-CeO2@rGO) composite has been synthesized by sonochemical method. The characterization of as prepared nanocomposite was intensely performed by UV-Vis, FT-IR, EDX, FE-SEM, HR-TEM, XRD, and TGA analysis. The synthesized nanomaterial was further investigated for its selective and sensitive sensing of paracetamol (PM) based on a N-CeO2@rGO modified glassy carbon electrode. A distinct and improved reversible redox peak of PM is obtained at N-CeO2@rGO nanocomposite compared to the electrodes modified with N-CeO2 and rGO. It displays a very good performance with a wide linear range of 0.05-0.600 mu M, a very low detection limit of 0.0098 mu M (S/N = 3), a high sensitivity of 268 A mu M-1 cm(-2) and short response time (< 3 s). Also, the fabricated sensor shows a good sensibleness for the detection of PM in various tablet samples.