• 文献标题:   Morphology, thermal and mechanical properties of epoxy adhesives containing well-dispersed graphene oxide
  • 文献类型:   Article
  • 作  者:   XUE G, ZHANG B, SUN MM, ZHANG XG, LI JH, WANG L, SONG CY
  • 作者关键词:   graphene oxide, dispersion, adhesive, mechanical properties of adhesive, thermal analysi
  • 出版物名称:   INTERNATIONAL JOURNAL OF ADHESION ADHESIVES
  • ISSN:   0143-7496 EI 1879-0127
  • 通讯作者地址:   Heilongjiang Acad Sci
  • 被引频次:   10
  • DOI:   10.1016/j.ijadhadh.2018.10.011
  • 出版年:   2019

▎ 摘  要

Graphene oxide (GO) is prepared and introduced into epoxy resins through a wet-transfer migration technique using a three-roll mill. The results of TEM, XRD and digital microscope observation show that good dispersion of GO is achieved without using any additives. The mechanical and thermal properties of GO/epoxy (GO/EP) adhesives are enhanced with GO incorporated. A 10.2% increase in Young's modulus and a 56.3% increase in elevated-temperature (120 degrees C) lap shear strength (LSS) was observed on addition of 1.0 wt% GO, compared to the neat epoxy adhesive. Increased glass transition temperature and improved thermal stability of the GO/EP adhesives are also observed in the DMA and TG analysis. Moreover, the toughness of the GO/EP adhesives is improved and much rougher fracture surface can be observed compared with the neat epoxy adhesive. No GO agglomeration can be observed in the SEM images of GO/EP adhesive with 1.0 wt% loading.