• 文献标题:   An electrochemical sensor based on clay/graphene oxide decorated on chitosan gel for the determination of flubendiamide insecticide
  • 文献类型:   Article
  • 作  者:   AGHRIS S, CHHAIBI B, OUATMANE FZ, ALAOUI OT, LAGHRIB F, FARAHI A, BAKASSE M, LOUKILI A, LAHRICH S, EL MHAMMEDI MA
  • 作者关键词:   thermally reduced graphene oxide, natural clay composite, flubendiamide, chemically modified electrode
  • 出版物名称:   MATERIALS CHEMISTRY PHYSICS
  • ISSN:   0254-0584 EI 1879-3312
  • 通讯作者地址:  
  • 被引频次:   1
  • DOI:   10.1016/j.matchemphys.2022.127243 EA DEC 2022
  • 出版年:   2023

▎ 摘  要

This paper presents a thermally reduced graphene/clay/chitosan modified pencil electrode for ultrasensitive detection of Flubendiamide using differential pulse voltammetry. The graphene oxide was synthesized by exfoliation of graphite with an eco-friendly procedure. The as-produced reduced graphene/clay/chitosan com-posite is characterized by utilizing Fourier transform infrared spectroscopy and Scanning electron microscopy. The electrochemical behavior of the electrode before and after modification was investigated by cyclic vol-tammetry. Under optimized conditions, the reduced graphene/clay/chitosan modified pencil electrode exhibited excellent analytical properties toward Flubendiamide determination using differential pulse voltammetry. A linear calibration curve was established from 0.02 to 15 mu mol L-1 for Flubendiamide with a limit of detection of 0.001 mu mol L-1. The method was effectively employed for Flubendiamide detection in white rice samples.