• 文献标题:   Single-step fiber laser reduction and patterning of graphene oxide films for ceramic-based heaters
  • 文献类型:   Article
  • 作  者:   TSENG SF, CHAO CT
  • 作者关键词:   singlestep reduction patterning, highpulse nanosecond fiber laser, reduced graphene oxide films rgofs, ceramicbased heater, xray photoelectron spectroscopy, oxygen functional group
  • 出版物名称:   CERAMICS INTERNATIONAL
  • ISSN:   0272-8842 EI 1873-3956
  • 通讯作者地址:  
  • 被引频次:   4
  • DOI:   10.1016/j.ceramint.2021.05.058 EA JUL 2021
  • 出版年:   2021

▎ 摘  要

A single-step reduction and patterning technique that involves high-pulse nanosecond fiber laser irradiation was used to reduce graphene oxide films (GOFs) for use in ceramic-based heaters. Laser reduction of GOFs was performed at a laser power, scan speed, pulse repetition frequency, and laser scan pitch of 2.2-4.1 W, 150-500 mm/s, 750 kHz, and 10 mu m, respectively. The optimal intensity ratios of the D to G band (RD/G) and the 2D to G band (R2D/G) of reduced GOFs (RGOFs), obtained from Raman spectra, were 0.251 and 0.587, respectively. Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy analyses revealed that oxygencontaining functional groups in RGOFs coated onto ceramic substrates were removed by increasing the average laser power and decreasing the laser scanning speed. Moreover, the typical RGOFs exhibited a lowest sheet resistance of 22.75 +/- 2.75 omega/, which was achieved with an average laser power and scan speed of 3.35 W and 300 mm/s, respectively. The highest temperature of the typical laser-patterned RGOFs was approximately 123.3 degrees C, which occurred when the RGOFs were produced using a laser power, scan speed, and applied direct current voltage of 3.27 W, 200 mm/s, and 10 V, respectively.