• 文献标题:   Dispersion of graphite flakes into boehmite sols for the preparation of bilayer-graphene / alumina coatings on stainless steel for tribological applications
  • 文献类型:   Article
  • 作  者:   HENTOUR K, TURQ V, WEIBEL A, ANSART F, SOBRINO JM, GARCIA J, CARDEY PF, LAURENT C
  • 作者关键词:   graphite, graphene, alumina, composite coating, tribology
  • 出版物名称:   JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
  • ISSN:   0955-2219 EI 1873-619X
  • 通讯作者地址:   Univ Toulouse 3 Paul Sabatier
  • 被引频次:   6
  • DOI:   10.1016/j.jeurceramsoc.2018.10.027
  • 出版年:   2019

▎ 摘  要

Carbon-alumina coatings on stainless steel were prepared by a sol-gel route. The dispersion of the commercial graphite flakes by an ultrasonic bath, an ultrasonic probe and a high-shear mixer, produce thinner flakes, fewlayered-graphene and bi-layer-graphene (BLG), respectively. The coatings were examined by optical and electron microscopy, interferential rugosimetry, optical profilometry and Raman spectroscopy. The friction coefficient against a steel ball is decreased by a factor of 5-7 and the wear volume is reduced by a factor of 6-38 compared to a pure alumina coating. The best results correspond to the sample prepared using the high-shear mixer. Delamination of the graphite flakes into BLG during the friction test provides the system with debris suitable for tribofilm building up and lubrication but it is better to already have carbon dispersed as BLG in the coating before the test, notably because the carbon surface area available is much higher.