• 文献标题:   Preparation, performance and mechanism of 3-aminopropyltriethoxysilane modified graphene oxide as nano shale swelling inhibitor
  • 文献类型:   Article, Early Access
  • 作  者:   WANG XY, DU WC, HU WC, ZHANG J, CHEN G
  • 作者关键词:   drilling fluid, hydration swelling, nano graphene, shale inhibitor
  • 出版物名称:   INORGANIC NANOMETAL CHEMISTRY
  • ISSN:   2470-1556 EI 2470-1564
  • 通讯作者地址:  
  • 被引频次:   0
  • DOI:   10.1080/24701556.2021.1987464 EA SEP 2021
  • 出版年:   2021

▎ 摘  要

Wellbore instability is a challenging technical problem in drilling operation, shale inhibitor can effectively inhibit shale hydration and dispersion, so as to stabilize the wellbore of shale. In this paper, graphene oxide was prepared by Hummer's method, and modified by 3-aminopropyltriethoxysilane. The structure of modified graphene oxide was characterized using FT-IR and TGA, and the results showed that modified graphene oxide has been successfully prepared. The inhibitive performance was investigated by the linear swelling and hot-rolling tests, which shows the swelling rate of artificial core is reduced by 10.32% in 2.0% inhibitor solutions and the shale rolling recovery rate was reached 90.13% in 3.0% inhibitor solutions at the rolling condition of 120 degrees C x 16 h. Finally, the inhibition mechanism was studied, inhibitor can enter into the interlayer of shale and change the appearance of bentonite by physical and chemical interaction, and in that way achieve a good inhibition result.