• 文献标题:   Ultrasound promoted facile one pot synthesis of triazole derivatives catalyzed by functionalized graphene oxide Cu(I) complex under mild conditions
  • 文献类型:   Article
  • 作  者:   NAEIMI H, SHAABANI R
  • 作者关键词:   ultrasound, 1 2 3triazole, graphene oxide, one pot, three component
  • 出版物名称:   ULTRASONICS SONOCHEMISTRY
  • ISSN:   1350-4177 EI 1873-2828
  • 通讯作者地址:   Univ Kashan
  • 被引频次:   22
  • DOI:   10.1016/j.ultsonch.2016.05.043
  • 出版年:   2017

▎ 摘  要

A facile one pot three component reaction of alkyl halides, sodium azide with terminal alkynes can be catalyzed by functionalized graphene oxide copper (I) complex under ultrasonic irradiation at room temperature. In this protocol, the 1,4-disubstituted 1,2,3-triazoles were afforded as target pure products in excellent yields and short reaction times. The prepared catalyst has been characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction spectroscopy (XRD), Energy Dispersive X-ray (EDX) and field emission scanning electron microscopy (FE-SEM) techniques. Also, the catalyst is chemoselective and stable and can be reused several times without any appreciable loss of its catalytic activity. (C) 2016 Elsevier B.V. All rights reserved.