• 文献标题:   Synthesis, characterization, morphology, and adsorption studies of ternary nanocomposite comprising graphene oxide, chitosan, and polypyrrole
  • 文献类型:   Article
  • 作  者:   KAMAL S, KHAN F, KAUSAR H, KHAN MS, AHMAD A, AHMAD SI, ASIM M, ALSHITARI W, NAMI SAA
  • 作者关键词:   adsorption, chitosan, graphene oxide, polypyrrole, ternary nanocomposite
  • 出版物名称:   POLYMER COMPOSITES
  • ISSN:   0272-8397 EI 1548-0569
  • 通讯作者地址:   Aligarh Muslim Univ
  • 被引频次:   2
  • DOI:   10.1002/pc.25673 EA JUN 2020
  • 出版年:   2020

▎ 摘  要

The present work reports the synthesis of a ternary nanocomposite GO-CS-PPy comprising of graphene oxide (GO), chitosan (CS), and polypyrrole (PPy). The ternary nanocomposite GO-CS-PPy was characterized by a variety of techniques like Fourier transform infrared spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction analysis (XRD), thermogravimetric analysis, and differential thermal analysis. Thein situsynthesis of ternary nanocomposite GO-CS-PPy was carried out in the presence of catalytic FeCl3. The SEM and TEM analyses reveal a clear transformation of GO into the nanocomposite form where the characteristic sheet-like structure of the former was crushed and converted into small pieces of nonuniform size. Similarly, in the XRD, the diagnostic peak of GO is also shifted appreciably employing successful synthesis of ternary nanocomposite GO-CS-PPy. The thermal stability of the ternary nanocomposite GO-CS-PPy was also found to be enhanced as compared to the pristine GO, CS, and PPy individually. The ternary nanocomposite GO-CS-PPy was used as an efficient adsorbent for the removal of a popular anionic dye Congo red as well as for the removal of heavy metal ions like Cu(2+)and Cd(2+)from water. In both cases, the ternary nanocomposite GO-CS-PPy was found to be very effective and can be commercialized in near future after further comprehensive studies.