• 文献标题:   Exfoliation of graphene sheets via high energy wet milling of graphite in 2-ethylhexanol and kerosene
  • 文献类型:   Article
  • 作  者:   ALSHERBINI AS, BAKR M, GHONEIM I, SAAD M
  • 作者关键词:   graphene, wet ball milling, kerosene, 2ethylhexanol, defect, raman spectroscopy
  • 出版物名称:   JOURNAL OF ADVANCED RESEARCH
  • ISSN:   2090-1232 EI 2090-1224
  • 通讯作者地址:   Cairo Univ
  • 被引频次:   12
  • DOI:   10.1016/j.jare.2017.01.004
  • 出版年:   2017

▎ 摘  要

Graphene sheets have been exfoliated from bulk graphite using high energy wet milling in two different solvents that were 2-ethylhexanol and kerosene. The milling process was performed for 60 h using a planetary ball mill. Morphological characteristics were investigated using scanning electron microscope (SEM) and transmission electron microscope (TEM). On the other hand, the structural characterization was performed using X-ray diffraction technique (XRD) and Raman spectrometry. The exfoliated graphene sheets have represented good morphological and structural characteristics with a valuable amount of defects and a good graphitic structure. The graphene sheets exfoliated in the presence of 2-ethylhexanol have represented many layers, large crystal size and low level of defects, while the graphene sheets exfoliated in the presence of kerosene have represented fewer number of layers, smaller crystal size and higher level of defects. (C) 2017 Production and hosting by Elsevier B.V. on behalf of Cairo University.This is an open access article under the CC BY-NC-ND license