• 文献标题:   Transformation of graphene oxide in supercritical media
  • 文献类型:   Article
  • 作  者:   GROSHKOVA YA, BUSLAEVA EY, GUBIN SP
  • 作者关键词:   graphene oxide, graphene, supercritical fluid, supercritical isopropyl alcohol, supercritical acetone, supercritical water
  • 出版物名称:   RUSSIAN CHEMICAL BULLETIN
  • ISSN:   1066-5285 EI 1573-9171
  • 通讯作者地址:   Russian Acad Sci
  • 被引频次:   0
  • DOI:  
  • 出版年:   2019

▎ 摘  要

Graphene oxide (GO) synthesized according to the modified Hummers method was reduced by supercritical isopropyl alcohol (SCI), supercritical acetone (SCA), and supercritical water (SCW). Methods free of toxic reducing agents were developed for the graphene production. The composition, morphology, and structure of synthesized graphene were determined using CHN analysis, XRD, Raman spectroscopy, and scanning electron microscopy. The best results were acquired in the case of GO reduction in SCA and SCI at high parameters.