• 文献标题:   Fabrication and physicochemical characterization of graphene oxide derived from thermally expanded graphite
  • 文献类型:   Article
  • 作  者:   ILKEVICH LV, TKACHENKO TB, SAMAROV AV, BURTSEV AA, SOZINOV SA, HITSOVA LM, POPOVA AN, BARNAKOV CN, KOZLOV AP
  • 作者关键词:   graphene oxide, expanded graphite, modified hummers method
  • 出版物名称:   RUSSIAN CHEMICAL BULLETIN
  • ISSN:   1066-5285 EI 1573-9171
  • 通讯作者地址:   Russian Acad Sci
  • 被引频次:   0
  • DOI:   10.1007/s11172-018-2168-6
  • 出版年:   2018

▎ 摘  要

Graphene oxide was obtained from expanded graphite according to the modified Hummers method. The reaction time was significantly reduced (from 24 to 8 h) by applying the expanded graphite in the oxidation process. The interlayer distance in obtained samples was equal to 0.70-0.74 nm. Structural features of the material were studied by the powder X-ray diffraction, thermogravimetric analysis, scanning electron microscopy, transmission electron microscopy, XPS spectroscopy, and NMR spectroscopy.