• 文献标题:   Graphene NanoPlatelets reinforced tantalum carbide consolidated by spark plasma sintering
  • 文献类型:   Article
  • 作  者:   NIETO A, LAHIRI D, AGARWAL A
  • 作者关键词:   ceramic, composite, sintering, fracture, nanoindentation
  • 出版物名称:   MATERIALS SCIENCE ENGINEERING ASTRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE PROCESSING
  • ISSN:   0921-5093 EI 1873-4936
  • 通讯作者地址:   Florida Int Univ
  • 被引频次:   89
  • DOI:   10.1016/j.msea.2013.06.006
  • 出版年:   2013

▎ 摘  要

Graphene NanoPlatelets (GNP) reinforced tantalum carbide composites are synthesized by spark plasma sintering (SPS) at processing conditions of 1850 degrees C and 80-100 MPa. The GNP addition enhances the densification of TaC-GNP composites to 99% theoretical density, while reducing the grain size by over 60% through grain wrapping mechanism. Survival and structure retention of GNP is confirmed through scanning electron microscopy and micro-Raman spectroscopy. Nanoindentation and high load (20-30 N) microindentation are utilized to evaluate elastic modulus and hardness. GNP improves fracture toughness of TaC by up to 99% through toughening mechanisms such as GNP bending, sheet sliding, cracking bridging, and crack deflection. (C) 2013 Elsevier B.V. All rights reserved.