• 文献标题:   Synthesis of nitrogen-doped graphene nanosheets decorated with gold nanoparticles as an improved sensor for electrochemical determination of chloramphenicol
  • 文献类型:   Article
  • 作  者:   BOROWIEC J, WANG R, ZHU LH, ZHANG JD
  • 作者关键词:   nitrogen doped graphene, gold nanoparticle, chloramphenicol, voltammetric analysi
  • 出版物名称:   ELECTROCHIMICA ACTA
  • ISSN:   0013-4686 EI 1873-3859
  • 通讯作者地址:   Huazhong Univ Sci Technol
  • 被引频次:   92
  • DOI:   10.1016/j.electacta.2013.03.092
  • 出版年:   2013

▎ 摘  要

Nitrogen-doped graphene nanosheets decorated with gold nanoparticles (Au/N-G) were synthesized by the reduction of HAuCl4 on the surface of N-G using ethylene glycol as the reducing agent. The surface characterization with various techniques such as scanning electron microscopy, X-ray diffraction and X-ray photoelectron spectroscopy showed that many gold nanoparticles were effectively loaded on the surface of N-G via the proposed synthesis process. The impedance analysis indicated that Au/N-G was an excellent electrode material possessing outstanding electrochemical features for electron transfer. Using Au/N-G modified electrode, the electrochemical response of chloramphenicol (CAP) was significantly increased due to the synergetic effect of two nanomaterials. Thus, a high-performance electrochemical sensor for CAP based on Au/N-G was developed. (C) 2013 Elsevier Ltd. All rights reserved.