• 文献标题:   Fast synthesis of methacrylated graphene oxide: a graphene-functionalised nanostructure
  • 文献类型:   Article
  • 作  者:   MAMAGHANI KR, NAGHIB SM, ZAHEDI A, KALKHORAN AHZ, RAHMANIAN M
  • 作者关键词:   graphene, nanostructured material, nanofabrication, ultraviolet spectra, visible spectra, fourier transform infrared spectra, raman spectra, field emission electron microscopy, transmission electron microscopy, atomic force microscopy, co, methacrylate group, functional group, afm, atomic force microscope, tem, transmission electron microscope, fesem, field emission scanning electron microscope, raman spectroscopy, ftir, fourier transform infrared spectroscopy, uvvis spectroscopy, modified hummer method, graphenefunctionalised nanostructure, methacrylated graphene oxide
  • 出版物名称:   MICRO NANO LETTERS
  • ISSN:   1750-0443
  • 通讯作者地址:   IUST
  • 被引频次:   3
  • DOI:   10.1049/mnl.2017.0461
  • 出版年:   2018

▎ 摘  要

Graphene oxide (GO) was successfully synthesised via modified Hummer method and functionalised by methacrylate named MeGO (metacrylated GO). Different characterisation methods containing UV-vis, Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, field emission scanning electron microscope (FESEM), transmission electron microscope (TEM) and atomic force microscope (AFM) analyses were employed to characterise the structure and morphology of MeGO. The outputs of the different analyses confirmed each other and proved the presence of the methacrylate functional group on the surface of the GO. Displacement in the peaks of UV-vis analysis coupled with the new peaks in FTIR results clearly demonstrated the creation of a new functional group. The G/D ratio of MeGO in Raman spectroscopy has increased to 1.17 and FESEM and TEM investigations confirmed the wrinkled structure of MeGO sheets. Also, it was observed that the distance between the GO layers was increased about 2.86 nm after functionalisation of GO layers by methacrylate groups. This nanomaterial with difference characterisation and specific properties in comparison with GO could be a great candidate for further developments in industrial and biomedical applications.