• 专利标题:   Preparing graphene involves using carbonate solution as electrolyte and graphite rod as anode and cathode, sleeving hollow quartz tube with graphite rod, and soaking graphite electrode in carbonate solution, electrode tip is set.
  • 专利号:   CN107459031-A
  • 发明人:   JI Y, LI H, LI J, XIONG D
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN107459031-A 12 Dec 2017 C01B-032/184 201803 Pages: 8 Chinese
  • 申请详细信息:   CN107459031-A CN10353062 25 May 2016
  • 优先权号:   CN10353062

▎ 摘  要

NOVELTY - Preparing graphene involves using 0.12 wt.% 0.24 grams/liter carbonate solution as electrolyte and graphite rod as anode and cathode. The hollow quartz tube is sleeved with graphite rod, where graphite electrode is dipped in the carbonate solution, where electrode tip is below liquid surface having distance of 2 plus minus 0.5 millimeter. The surface is treated at 0-10 degrees C and 1.30-1.80 kiloVolt to generate glow discharge. The solution is evaporated partially and dialyzed to to neutral, which is frozen and dried to obtain graphene. USE - Method for preparing graphene as automobile lubricating oil additive (claimed). ADVANTAGE - The method enables to prepare graphene reduces friction and abrasion, prolongs the service life and reduces the energy consumption.