• 专利标题:   Preparing graphene material using ball milling comprises e.g. ball milling graphite carbon, alkylated six-membered aromatic ring or fused ring polyether nonionic surfactant and deionized water in ball mill, and adding into deionized water.
  • 专利号:   CN103466608-A, CN103466608-B
  • 发明人:   LIU H, MAO M
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103466608-A 25 Dec 2013 C01B-031/04 201419 Pages: 6 Chinese
  • 申请详细信息:   CN103466608-A CN10411516 11 Sep 2013
  • 优先权号:   CN10411516

▎ 摘  要

NOVELTY - Preparing graphene material using ball milling comprises (i) mixing graphite carbon, alkylated six-membered aromatic ring or fused ring polyether nonionic surfactant and deionized water in a ball mill according to ratio of 1:2-1:15, and ball milling for 5-30 hours under ball milling speed of 200-500 rotation/minute; and (ii) adding the product obtained in the step (i) into deionized water, centrifuging for 10-30 minutes under centrifugal speed of 3000-8000 rotation/minute to obtain black upper layer colloidal suspension, and obtaining aqueous graphene solution with different concentrations. USE - The method is useful for preparing graphene material using ball milling (claimed). ADVANTAGE - The method: utilizes the ball mill, which is simple, easy to operate and safe; is simple; has mild reaction condition and large yield. The graphene material is environmentally friendly.