• 专利标题:   Preparing electrified bismuth trisulfide nanorod RGO composite structure comprises e.g. dissolving soluble bismuth salt in homologous acid solution, dispersing graphene oxide in deionized water, and adding colourless transparent solution.
  • 专利号:   CN105417579-A
  • 发明人:   MAO L, WANG L
  • 专利权人:   SENSONG JIANGSU HEAVY IND CO LTD
  • 国际专利分类:   B82Y030/00, C01B031/04, C01G029/00
  • 专利详细信息:   CN105417579-A 23 Mar 2016 C01G-029/00 201638 Pages: 5 English
  • 申请详细信息:   CN105417579-A CN10776617 16 Nov 2015
  • 优先权号:   CN10776617

▎ 摘  要

NOVELTY - Preparing electrified bismuth trisulfide nanorod RGO composite structure comprises (i) taking soluble bismuth salt, and dissolving in homologous acid solution to obtain colorless transparent solution, (ii) taking graphene oxide dispersing in deionized water, and adding colourless transparent solution to obtain black mixed solution, (iii) adding thioacetamide, allowing to stand to obtain black flocculent precipitate, and washing, (iv) dispersing the product in hydrazine hydrate solution, and stirring to obtain black precipitate, (v) purifying black precipitate, washing, and vacuum drying. USE - The method is useful for preparing electrified bismuth trisulfide nanorod RGO composite structure (claimed). ADVANTAGE - The composite structure has good electrochemical performance. DETAILED DESCRIPTION - Preparing electrified bismuth trisulfide nanorod RGO composite structure comprises (i) taking 2 mmol soluble bismuth salt, and dissolving in 50 ml homologous acid solution to obtain colorless transparent solution, (ii) taking 5-10 mg graphene oxide ultrasonically dispersing in 50 ml deionized water, and adding colourless transparent solution obtained in the step (i), obtain black mixed solution, (iii) taking black mixed solution obtained in the step (ii), adding 5 mmol thioacetamide, allowing to stand for 24-48 hours to obtain black flocculent precipitate, taking out black flocculent precipitate, and washing using deionized water to a pH value of 7, (iv) taking the product obtained in the step (iii), dispersing in 50% hydrazine hydrate solution, and continuously stirring for 8-12 hours using magnetic force stirrer to obtain black precipitate, (v) taking the black precipitate obtained in the step (iv), purifying by centrifugation, first washing for 3 times with ethanol, then washing for 3 times using deionized water, and carrying out vacuum drying at 70 degrees C for 4-6 hours to obtain electrified bismuth trisulfide nanorod RGO composite structure.