• 专利标题:   Preparing modified graphene ultraviolet absorbing agent, comprises dissolving cyanuric chloride in tetrahydrofuran, reacting with anhydrous aluminum chloride and resorcinol, adding chlorobenzene solvent, and reacting with epoxy chloropropane, potassium carbonate and dimethylformamide.
  • 专利号:   CN115650961-A
  • 发明人:   RAN M, FU X, ZHAO L, HUANG Z, XU W, FAN X
  • 专利权人:   CHINA BLUESTAR CHENGRAND RES CHEM IND, ZHONGLAN CHENGUANG CHEM CO LTD
  • 国际专利分类:   C07D405/10, C09K015/30, D06M101/36, D06M013/364
  • 专利详细信息:   CN115650961-A 31 Jan 2023 C07D-405/10 202319 Chinese
  • 申请详细信息:   CN115650961-A CN11211634 30 Sep 2022
  • 优先权号:   CN11211634

▎ 摘  要

NOVELTY - Preparing modified graphene ultraviolet absorbing agent, comprises (i) adding cyanuric chloride in 80 pts. wt. tetrahydrofuran (THF), stirring and dissolving, taking oxidation graphene sodium hydroxide and THF to prepare THF slurry, stirring, dripping prepared solution of THF and cyanuric chloride into THF slurry, reacting for 2-8 hours at 30-40℃, evaporating THF, adding water, filtering, water washing filter cake, vacuum drying to obtain the product I, (ii) adding chlorobenzene into 5 pts. wt. product I, adding anhydrous aluminum chloride and resorcinol, reacting for 3-8 hours at 70-80℃, adding water with chlorobenzene solvent, heating and refluxing, separating out ochlorobenzene, filtering, water washing filter cake, vacuum drying to obtain the product II, and (iii) taking product II, reacting epoxy chloropropane, potassium carbonate and Dimethylformamide (DMF) at 80-90℃ for 3-5 hours, cooling, filtering, washing, and drying. USE - The method is useful for preparing modified graphene ultraviolet absorbing agent. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for modified graphene ultraviolet absorbing agent prepared by above mentioned method.