• 专利标题:   Preparation of graphene-carbon nanotube pure carbon composite film by taking copper foil as substrate, preparing graphene thin film by atmospheric pressure chemical vapor deposition, and adding carbon nanotube powder into o-dichlorobenzene.
  • 专利号:   CN106276870-A
  • 发明人:   FU Z, HUANG W, WANG C, ZHU J, ZHAO H, MI R
  • 专利权人:   LASER FUSION RES CENT CHINA ACAD ENG PHY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106276870-A 04 Jan 2017 C01B-031/04 201713 Pages: 16 Chinese
  • 申请详细信息:   CN106276870-A CN10600088 27 Jul 2016
  • 优先权号:   CN10600088

▎ 摘  要

NOVELTY - Preparation of graphene-carbon nanotube pure carbon composite film includes taking copper foil as substrate, preparing graphene thin film by atmospheric pressure chemical vapor deposition, adding carbon nanotube powder into o-dichlorobenzene, mixing, putting in ultrasonic cleaning machine, continuously ultrasonically processing to obtain carbon nanotube dispersion liquid, uniformly dispersing on graphene film by titration, placing in tubular furnace, heat treating under inert atmosphere to remove the solvent, and obtaining copper foil-graphene-carbon nanotube material. USE - Preparation of graphene-carbon nanotube pure carbon composite film used in FETs and laser fields. ADVANTAGE - The method provides graphene-carbon nanotube pure carbon composite film with light transmittance and good conductivity. DETAILED DESCRIPTION - Preparation of graphene-carbon nanotube pure carbon composite film comprises taking copper foil as substrate, preparing graphene thin film by atmospheric pressure chemical vapor deposition, adding carbon nanotube powder into o-dichlorobenzene, mixing, putting in ultrasonic cleaning machine, continuously ultrasonically processing to obtain carbon nanotube dispersion liquid, uniformly dispersing on graphene film by titration, placing in tubular furnace, heat treating under inert atmosphere to remove the solvent, obtaining copper foil-graphene-carbon nanotube material, subjecting to particle beam irradiation, etching by etching solution to remove copper foil, washing the residual etching solution with deionized water, and obtaining the product.