• 专利标题:   Preparation of composite material involves dispersing nitrogen-containing graphene oxide in water to form uniform suspension, adding obtained manganese dioxide-coated sulfur particles, stirring, suction filtering, and washing.
  • 专利号:   WO2018184156-A1
  • 发明人:   ZHONG L
  • 专利权人:   SHENZHEN PEICHENG TECHNOLOGY CO LTD
  • 国际专利分类:   B82Y030/00, H01M010/052, H01M004/36, H01M004/38, H01M004/62
  • 专利详细信息:   WO2018184156-A1 11 Oct 2018 H01M-004/36 201871 Pages: 15 Chinese
  • 申请详细信息:   WO2018184156-A1 WOCN079505 05 Apr 2017
  • 优先权号:   WOCN079505

▎ 摘  要

NOVELTY - Preparation of nitrogen-doped graphene/manganese dioxide/hollow sulfur composite material involves stirring sulfur powder and carbon disulfide to form a uniform solution, ball milling high purity nickel powder for 0.5-2 hours, adding nickel powder into the solution, stirring to form a uniform suspension, stirring for 0.5-1 hour, spray drying to form sulfur-coated spherical particles, stirring spherical particles and ferric chloride solution for 1-5 hours, washing using water, filtering, adding filtered precipitate into a solution containing manganese chloride and potassium permanganate, stirring to form a uniform suspension, heating, stirring, reacting at 50-70 degrees C for 5-30 minutes, centrifuging, washing using water to obtain manganese dioxide-coated sulfur particles, adding nitrogen-containing graphene oxide into water, ultrasonically dispersing to form a uniform suspension, adding manganese dioxide-coated sulfur particles, stirring for 5-30 minutes, suction filtering, and washing. USE - Preparation of nitrogen-doped graphene/manganese dioxide/hollow sulfur composite material. ADVANTAGE - The prepared composite material has improved electrochemical properties.