• 专利标题:   Separating graphene oxide flakes by gradient fractionation comprises producing density gradient by ultracentrifugation in solution of sodium chloride and percoll and placing a layer on surface of generated gradient graphene oxide.
  • 专利号:   PL414340-A1, PL227355-B1
  • 发明人:   MIJOWSKA E, URBAS K
  • 专利权人:   UNIV ZACHODNIOPOMORSKI TECHNOLOGICZNY
  • 国际专利分类:   B03B005/32, C01B032/198
  • 专利详细信息:   PL414340-A1 24 Apr 2017 201814 Pages: 1
  • 申请详细信息:   PL414340-A1 PL414340 13 Oct 2015
  • 优先权号:   PL414340

▎ 摘  要

NOVELTY - Separating graphene oxide flakes by gradient fractionation comprises producing density gradient by ultracentrifugation for 60 minutes at 40000 revolutions in solution of 0.15 M sodium chloride and percoll in a 1: 1 volume ratio, placing a layer on the surface of the generated gradient graphene oxide previously dispersed in water using an ultrasonic probe, after which the mixture is subjected to ultracentrifugation for 10-12 minutes at 20000- 22000 revolutions minutes, collecting resulting fractions, placing in separate containers with pipette and purifying. USE - The method is useful for separating graphene oxide flakes by gradient fractionation. DETAILED DESCRIPTION - Separating graphene oxide flakes by gradient fractionation comprises producing density gradient by ultracentrifugation for 60 minutes at 40000 revolutions in solution of 0.15 M sodium chloride and percoll in a 1: 1 volume ratio, placing a layer on the surface of the generated gradient graphene oxide previously dispersed in water using an ultrasonic probe, after which the mixture is subjected to ultracentrifugation for 10-12 minutes at 20000- 22000 revolutions minutes, collecting resulting fractions, placing in separate containers with pipette, purifying the obtained products by exposure to concentrated hydrofluoric acid, washed several times with water and dried in a vacuum at 100 degrees C.