• 专利标题:   Preparation of micro-nano structured graphene powder by hydrothermally synthesizing urchin-like cobalt hydroxide powder, soaking in dimethylformamide solution of polymethyl methacrylate, drying, annealing and steeping with hydrochloric acid.
  • 专利号:   CN105060284-A, CN105060284-B
  • 发明人:   DONG J, HE H, LI K, WANG H, ZENG X
  • 专利权人:   UNIV YANGZHOU
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN105060284-A 18 Nov 2015 C01B-031/04 201612 Pages: 5 English
  • 申请详细信息:   CN105060284-A CN10501600 14 Aug 2015
  • 优先权号:   CN10501600

▎ 摘  要

NOVELTY - Preparation of micro-nano structured graphene powder comprises hydrothermally synthesizing urchin-like cobalt hydroxide powder, soaking in 0.5-2% dimethylformamide solution of polymethyl methacrylate for not less than 20 minutes, taking out, drying, annealing at 700-1100 degrees C under hydrogen atmosphere for more than 2 minutes to obtain black powder, steeping with diluted hydrochloric acid solution for more than 24 hours, and drying. USE - Method for preparing micro-nano structured graphene powder (claimed). ADVANTAGE - The graphene powder has high crystal quality, simple preparation method, low cost, and controllable and easy synthesis.