• 专利标题:   Preparation of graphene thermally conductive film involves coating slurry prepared by dissolving graphene oxide powder in solvent, and defoaming resultant, on substrate, drying, winding, trimming, heating, cooling, and vacuum rolling.
  • 专利号:   CN108203091-A, WO2018133338-A1, CN108203091-B, US2019031513-A1, KR2019070944-A
  • 发明人:   ZHOU B, ZHOU R, LI F, LU J
  • 专利权人:   HANGZHOU FUXI TECHNOLOGY CO LTD, CHANGZHOU FUXI TECHNOLOGY CO LTD, CHANGZHOU FUXI TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/192, C01B032/194, C01B032/184, C09K005/14, F28F021/02, H05K009/00
  • 专利详细信息:   CN108203091-A 26 Jun 2018 C01B-032/192 201853 Pages: 8 Chinese
  • 申请详细信息:   CN108203091-A CN10057914 23 Jan 2017
  • 优先权号:   CN10057914

▎ 摘  要

NOVELTY - Preparation of graphene thermally conductive film involves dissolving graphite oxide in 40-60 wt.% water, processing using a screw extruder, cutting into pellets to obtain graphite oxide particles having a particle size of 1-5 mm, subjecting to high-temperature stripping process in a high-temperature furnace in nitrogen or argon atmosphere at 800-1500 degrees C, obtaining graphene oxide powder, dissolving resultant in a solvent, defoaming resultant slurry, coating resultant slurry on a substrate by blade coating or extrusion coating method, drying in an oven at 70-150 degrees C to remove solvent, winding into coil, peeling resultant from the substrate using a stripping device, trimming using a trimming device, forming a continuous graphene oxide film web, placing in hot air oven, heating to 150-500 degrees C, cooling, heating to 2200-2800 degrees C, and vacuum rolling at 10-30 MPa. The substrate is steel strip, polyethylene terephthalate, 500-2000 mesh stainless steel mesh or 500-1000 mesh nylon mesh. USE - Preparation of graphene thermally conductive film. ADVANTAGE - The method enables efficient, continuous and economical preparation of graphene thermally conductive film with reduced energy consumption and without drying graphite oxide. DETAILED DESCRIPTION - The substrate has a thickness of 0.8-3 mm.