• 专利标题:   Method for preparing perovskite and graphene composite material that is utilized as e.g. lithium-air battery cathode, involves diluting graphene material, adding with citric acid and alkyl phenol polyoxyethylene ether, heating precursor.
  • 专利号:   CN105186011-A, CN105186011-B
  • 发明人:   LV W
  • 专利权人:   UNIV SHENZHEN
  • 国际专利分类:   H01M012/06, H01M004/90, H01M004/96
  • 专利详细信息:   CN105186011-A 23 Dec 2015 H01M-004/90 201617 Pages: 8 English
  • 申请详细信息:   CN105186011-A CN10336069 17 Jun 2015
  • 优先权号:   CN10336069

▎ 摘  要

NOVELTY - A perovskite and graphene composite material preparation method involves diluting graphene material in distilled water to obtain graphene suspension with concentration of 0.3-0.5mg/mL. The graphene suspension is added with nitrate and dispersed ultrasonically for 1-2 hours to obtain mixed solution. The resultant solution is added with citric acid and alkyl phenol polyoxyethylene ether. The pH of the solution is regulated to 8-10 by adding ammonia to obtain graphene/titanium precursor solution. The precursor solution is heated, dried and calcined. USE - Method for preparing perovskite and graphene composite material that is utilized as lithium-air battery cathode and dual-functional catalyst (claimed), and in mobile electronic devices and electric car batteries. ADVANTAGE - The method enables preparing the material with better battery charge and discharge performance, and durability. DETAILED DESCRIPTION - A perovskite and graphene composite material preparation method involves diluting graphene material in distilled water to obtain graphene suspension with concentration of 0.3-0.5mg/mL. The graphene suspension is added with nitrate and dispersed ultrasonically for 1-2 hours to obtain mixed solution. The resultant solution is added with citric acid and alkyl phenol polyoxyethylene ether. The pH of the solution is regulated to 8-10 by adding ammonia to obtain graphene/titanium precursor solution. The precursor solution is heated to 50-70 degrees C for 20-28h, dried and calcined to prepare lanthanum strontium manganite (La-1-xSrxMnO3) and graphene composite material, where x is 0-1. An INDEPENDENT CLAIM is also included for a perovskite and graphene composite material prepared by the method.