• 专利标题:   Preparation of bowl-shaped graphene/polypyrrole supercapacitor electrode material for energy device of flexible microelectronic device, involves performing electrodeposition of pyrrole monomer and lithium perchlorate deposition electrolyte.
  • 专利号:   CN111986932-A
  • 发明人:   XUE W, KONG K, ZHAO R, ZHU W
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/36, H01G011/48, H01G011/86
  • 专利详细信息:   CN111986932-A 24 Nov 2020 H01G-011/86 202004 Pages: 10 Chinese
  • 申请详细信息:   CN111986932-A CN10853751 21 Aug 2020
  • 优先权号:   CN10853751

▎ 摘  要

NOVELTY - Preparation of bowl-shaped graphene/polypyrrole supercapacitor electrode material involves cutting commercial graphite sheet as an anode into ammonium persulfate electrolyte, providing graphite electrode as cathode, modifying cross-section of graphite fiber by applying voltage, obtaining three-dimensional graphene, washing with deionized water and anhydrous ethanol, drying, carrying out electrodeposition of pyrrole monomer and lithium perchlorate deposition electrolyte using three-dimensional graphene as a working electrode, platinum electrode as counter electrode, and saturated calomel electrode as reference electrode, uniformly growing layer of polypyrrole on surface of three-dimensional graphene to form a unique bowl-shaped structure, washing with anhydrous ethanol and deionized water, placing in a vacuum oven for drying, and cutting into any required size. USE - Preparation of bowl-shaped graphene/polypyrrole supercapacitor electrode material used for energy device of flexible microelectronic device. ADVANTAGE - The method enables preparation of bowl-shaped graphene/polypyrrole supercapacitor electrode material having excellent capacity, rate characteristics, cycle characteristics, and electrochemical performance for long period of time, and improved volume expansion effect during charging and discharging. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for method for adjusting size and wall thickness of bowl of bowl-shaped graphene/polypyrrole supercapacitor electrode material.