• 专利标题:   Large reaction kettle useful for industrial preparation of graphene, comprises e.g. shaft sealing device, transmission device, protective support frame, gas collecting bottle, reaction bottle, constant temperature groove and feeding port.
  • 专利号:   CN102744028-A
  • 发明人:   DING R, GUO X, NI Z
  • 专利权人:   TAIZHOU JUNA NEW ENERGY CO LTD
  • 国际专利分类:   B01J019/18, B01J004/00, C01B031/04
  • 专利详细信息:   CN102744028-A 24 Oct 2012 B01J-019/18 201328 Pages: 5 Chinese
  • 申请详细信息:   CN102744028-A CN10207286 21 Jun 2012
  • 优先权号:   CN10207286

▎ 摘  要

NOVELTY - Large reaction kettle comprises a shaft sealing device, a transmission device, a protective support frame and a gas collecting bottle. The support frame is provided with a reaction bottle, which is connected with a constant temperature groove. The upper part of the reaction bottle is provided with a feeding port and a tail gas discharge port, and the lower part is provided with a lower port. The reaction bottle is a double-layered structure, and its middle part is provided with an interlayer, and is equipped with a variable frequency speed regulation stirrer and a temperature measuring pipe. USE - The reaction kettle is useful for industrial preparation of graphene. ADVANTAGE - The reaction kettle: utilizes multiple feeding ports to avoid contamination between the different raw materials; and has large volume and compact structure; and is a suitable container for large amount of physical and chemical reactions. DETAILED DESCRIPTION - Large reaction kettle comprises a shaft sealing device, a transmission device, a protective support frame (2) and a gas collecting bottle. The support frame is provided with a reaction bottle (1), which is externally connected with a constant temperature groove (3). The upper part of the reaction bottle is provided with a feeding port (4) and a tail gas discharge port (5), and the lower part is provided with a lower port. The reaction bottle is a double-layered structure, and its middle part is provided with an interlayer, and is equipped with a variable frequency speed regulation stirrer and a temperature measuring pipe. The regulation stirrer is provided with a tachometer with digital display. The temperature measuring pipe is provided with a digital display temperature controller. The tail gas discharge port is connected with the gas collecting bottle through a condensing pipe. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic representation of the large reaction kettle. Reaction bottle (1) Protective support frame (2) Constant temperature groove (3) Feeding port (4) Tail gas discharge port (5)