• 专利标题:   Aza-graphene fiber useful in the field of wearable electronic device, prepared by e.g. continuously wet spinning graphene oxide dispersion, soaking graphene oxide fiber in coagulation bath and subjecting fiber to hydrothermal treatment.
  • 专利号:   CN108914251-A
  • 发明人:   GAO C, CHU X
  • 专利权人:   HANGZHOU GAOXI TECHNOLOGY CO LTD, UNIV ZHEJIANG
  • 国际专利分类:   D01F009/12, D01D005/06
  • 专利详细信息:   CN108914251-A 30 Nov 2018 D01F-009/12 201908 Pages: 6 Chinese
  • 申请详细信息:   CN108914251-A CN10746197 09 Jul 2018
  • 优先权号:   CN10746197

▎ 摘  要

NOVELTY - Aza-graphene fiber, is claimed. The fiber is doped with pyrrole nitrogen, where the doping concentration is 7.92-7.98%. USE - The fiber is useful in the field of wearable electronic device. ADVANTAGE - The fiber assembled in supercapacitor has a capacity of up to 230 F/g. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing aza-graphene fiber, comprising (i) continuously wet spinning 10-20 mg/g graphene oxide dispersion; (ii) soaking the obtained graphene oxide fiber in a coagulation bath for more than 0.5 hour, where the coagulation bath is composed of ammonium bicarbonate ,water and ethanol in a mass ratio of 3-10:100:20; (iii) subjecting graphene oxide fiber to hydrothermal treatment in a hydrothermal kettle filled with of ammonium bicarbonate aqueous solution, where the temperature of the hydrothermal treatment is 180 degrees C and time is 0.5-18 hours, and the mass ratio of ammonium bicarbonate in ammonium bicarbonate aqueous solution and water is 1:10; (iv) washing using deionized water to obtain the product in reduction state.