• 专利标题:   Brazing of graphene composite interlayer of three-dimensional structure involves pre-treating foam metal, placing in deposition chamber, purging methane and argon, depositing, cooling, placing solder, brazing, heating and cooling.
  • 专利号:   CN104625283-A, CN104625283-B
  • 发明人:   FENG J, LIN J, LUO D, QI J, ZHANG T, TAN X
  • 专利权人:   HARBIN INST TECHNOLOGY, HARBIN INST TECHNOLOGY
  • 国际专利分类:   B23K001/008, B23K001/20, C23C016/26
  • 专利详细信息:   CN104625283-A 20 May 2015 B23K-001/008 201602 Pages: 7 Chinese
  • 申请详细信息:   CN104625283-A CN10828186 26 Dec 2014
  • 优先权号:   CN10828186

▎ 摘  要

NOVELTY - Brazing of graphene composite interlayer of three-dimensional structure involves ultrasonically pre-treating foam metal chosen from nickel and copper, using acetone, removing impurities, placing pretreated product in chemical vapor deposition chamber, purging methane and argon, depositing, cooling, forming three-dimensional structure of graphene metal composite, placing solder in intermediate layer of three-dimensional structure between to-be-welded surfaces, placing resultant product in vacuum brazing furnace, heat-preserving and cooling. USE - Brazing of graphene composite interlayer of three-dimensional structure (claimed). DETAILED DESCRIPTION - Brazing of graphene composite interlayer of three-dimensional structure involves ultrasonically pre-treating foam metal chosen from nickel and copper, using acetone for 10-20 minutes, removing impurities on foam metal surface, placing pretreated product in chemical vapor deposition chamber, evacuating to 20 Pa or less, purging argon at flow rate of 10-50 sccm, adjusting chamber pressure to 50-300 Pa, heating to 800-1200 degrees C, purging methane at flow rate of 5-40 sccm and argon at 60-95 sccm, respectively, adjusting pressure to 200-800 Pa, controlling deposition temperature to 800-1000 degrees C, depositing for 5-35 minutes, cooling to room temperature at cooling rate of 5-30 degrees C/minute, forming three-dimensional structure of graphene metal composite, placing solder in intermediate layer of three-dimensional structure between to-be-welded surfaces, placing resultant product in vacuum brazing furnace, heat-preserving at 500-1200 degrees C for 2-30 minutes and cooling to room temperature at cooling rate of 2-30 degrees C/minute.