• 专利标题:   Preparing amino-functionalized magnetic oxide graphene comprises e.g. dispersing graphene oxide and iron(II,III) oxide nanoparticles in water, ultrasonically dispersing to obtain mixture; and adding mixture to three-necked flask.
  • 专利号:   CN110368901-A
  • 发明人:   YANG W, BAO S, YU Y
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   B01J020/20, B01J020/28, B01J020/30, B01J020/34, C02F001/28, C02F101/22
  • 专利详细信息:   CN110368901-A 25 Oct 2019 B01J-020/20 201990 Pages: 13 Chinese
  • 申请详细信息:   CN110368901-A CN10773421 21 Aug 2019
  • 优先权号:   CN10773421

▎ 摘  要

NOVELTY - Preparing amino-functionalized magnetic oxide graphene comprises (1) dispersing graphene oxide and iron(II,III) oxide nanoparticles in water, and ultrasonically dispersing to obtain mixture; (2) adding the mixture to three-necked flask, heating to 35-60 degrees C, adding 3-aminopropyltriethoxysilane under stirring, reacting at 35-60 degrees C for 0.5-2 hours; adding mixture of glutaraldehyde and polyethyleneimine, reacting at 35-60 degrees C for 10-12 hours, and cooling to room temperature after completion of reaction; and (3) washing the product with water, freezing and drying. USE - The amino-functionalized magnetic oxide graphene useful for removing hexavalent chromium from sewage (claimed). ADVANTAGE - The amino-functionalized magnetic oxide graphene: has hexavalent chromium removal rate of 95-99.9%; can reduces hexavalent chromium in the sewage to below 0.004 mg/l; and is used in field of chromium-containing wastewater treatment. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) amino-functionalized magnetic oxide graphene useful for removing hexavalent chromium from sewage; and (2) regenerating amino-functionalized magnetic oxide graphene comprising preparing 0.1-0.5 mol/l sodium hydroxide solution to obtain regeneration liquid, soaking the amino-functionalized magnetic oxide graphene in regeneration liquid for 1-2 hours to complete regeneration.