• 专利标题:   Preparing graphene waterproof and cooling architectural coating comprises e.g. heating kaolin, cooling to prepare metakaolin, ball milling metakaolin, mixing metakaolin powder, sodium silicate and water, and mixing geopolymer slurry.
  • 专利号:   CN112538299-A
  • 发明人:   HAO Y, LU H, XU H
  • 专利权人:   NANTONG JINGRUI NEW CARBON MATERIAL TECHNOLOGY CO LTD
  • 国际专利分类:   C09D001/00, C09D125/14, C09D133/04, C09D007/61
  • 专利详细信息:   CN112538299-A 23 Mar 2021 C09D-133/04 202144 Pages: 5 Chinese
  • 申请详细信息:   CN112538299-A CN11630789 31 Dec 2020
  • 优先权号:   CN11630789

▎ 摘  要

NOVELTY - Preparing graphene waterproof and cooling architectural coating comprises (i) heating kaolin to 800-900 degrees C at the rate of 5-8 degrees C/minute for 2 hours, and cooling with the furnace temperature to prepare metakaolin, (ii) ball milling the metakaolin obtained in step (i) in planetary ball mill to a particle size less than or equal to 75 mu m, (iii) mixing the metakaolin powder, sodium silicate, and water obtained from step (ii) at a mass ratio of 50:10-20:30-40, using a high-speed mixer to stir for 10-20 minutes at a rate of 3000 revolutions per minute to prepare a geopolymer slurry, (iv) mixing the geopolymer slurry and building emulsion obtained from step (iii) at a mass ratio of 1:1, and using a high-speed mixer to stir at a rate of 400 revolutions per minute for 30-60 minutes to prepare a geopolymer-building emulsion composite base material, and (c) adding dispersant, defoamer, anti-mold agent, film-forming aid, cellulose ether, and graphene to the geopolymer-building emulsion composite base material. USE - The method is useful for preparing graphene waterproof and cooling architectural coating. ADVANTAGE - The method: improves weather resistance of the coating, durability and water resistance, and infrared emission rate of the coating layer; and realizes excellent energy-saving and waterproof effect. DETAILED DESCRIPTION - Preparing graphene waterproof and cooling architectural coating comprises (i) heating kaolin to 800-900 degrees C at the rate of 5-8 degrees C/minute for 2 hours, and cooling with the furnace temperature to prepare metakaolin, (ii) ball milling the metakaolin obtained in step (i) in planetary ball mill to a particle size less than or equal to 75 mu m, (iii) mixing the metakaolin powder, sodium silicate, and water obtained from step (ii) at a mass ratio of 50:10-20:30-40, using a high-speed mixer to stir for 10-20 minutes at a rate of 3000 revolutions per minute to prepare a geopolymer slurry, (iv) mixing the geopolymer slurry and building emulsion obtained from step (iii) at a mass ratio of 1:1, and using a high-speed mixer to stir at a rate of 400 revolutions per minute for 30-60 minutes to prepare a geopolymer-building emulsion composite base material, and (c) adding dispersant, defoamer, anti-mold agent, film-forming aid, cellulose ether, and graphene sequentially to the geopolymer-building emulsion composite base material, stirring at 400 revolutions per minute for 10-20 minutes, adding hollow glass beads and stirring at low speed for 20-30 minutes to obtain the finished product.