• 专利标题:   Preparing modified three dimensional graphene foam involves performing reaction with cyclohexane, polystyrene, graphene oxide and sodium dodecyl sulfate.
  • 专利号:   CN105600777-A, CN105600777-B
  • 发明人:   QU L, ZHANG P, ZHAO Y
  • 专利权人:   BEIJING INST TECHNOLOGY
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN105600777-A 25 May 2016 C01B-031/04 201666 Pages: 17 English
  • 申请详细信息:   CN105600777-A CN10066486 29 Jan 2016
  • 优先权号:   CN10066486

▎ 摘  要

NOVELTY - Preparing modified three dimensional graphene foam involves adding cyclohexane solution and polystyrene solution to 5-14 mg/mL solution of graphene oxide with stirring at 3000-6000 revolutions/minute followed by addition of sodium dodecyl sulfate and stirring is continued for 5-20 minutes to obtain a uniform mixed solution. The mixed solution is frozen in liquid nitrogen to obtain polystyrene modified graphene hydrogel which is lyophilized to obtain a polyphenylene ethylene-modified three-dimensional graphene airgel. USE - Method for preparing modified three dimensional graphene foam (claimed). ADVANTAGE - The method enables to prepare polyphenylene modified three-dimensional graphene foam in a simple and easy manner suitable for large-scale production. The product has a honeycomb shape structure with excellent electrochemical property. DETAILED DESCRIPTION - Preparing modified three dimensional graphene foam involves adding cyclohexane solution and polystyrene solution to 5-14 mg/mL solution of graphene oxide with stirring at 3000-6000 revolutions/minute followed by addition of sodium dodecyl sulfate and stirring is continued for 5-20 minutes to obtain a uniform mixed solution. The mixed solution is frozen in liquid nitrogen to obtain polystyrene modified graphene hydrogel which is lyophilized to obtain a polyphenylene ethylene-modified three-dimensional graphene airgel which under protective atmosphere of argon gas is annealed at 200 degrees C for 1-2 hours to obtain polyphenylene modified three-dimensional graphene foam.