• 专利标题:   Preparation of enzyme catalyzed three-dimensional porous graphene-carbon nanotube electrode involves mixing graphene oxide solution and carbon nanotube, stirring, reacting, freeze-drying, immersing and ultrasonically processing.
  • 专利号:   CN107565140-A
  • 发明人:   YANG X, FAN S, SHEN L, CHEN L, WANG H, WU M, DENG Z, LIU J, SU B
  • 专利权人:   UNIV WUHAN TECHNOLOGY
  • 国际专利分类:   H01M004/86, H01M004/88, H01M004/90
  • 专利详细信息:   CN107565140-A 09 Jan 2018 H01M-004/90 201816 Pages: 9 Chinese
  • 申请详细信息:   CN107565140-A CN11050393 31 Oct 2017
  • 优先权号:   CN11050393

▎ 摘  要

NOVELTY - Preparation of enzyme catalyzed three-dimensional porous graphene-carbon nanotube electrode involves mixing graphene oxide solution and a carbon nanotube, stirring for 1-2 hours, placing the mixed solution in a reactor and reacting for 160-180 degrees C for 10-12 hours to obtain a hydrogel and freeze-drying to obtain powdery three-dimensional porous composite material, immersing the composite material in N,N-dimethylformamide and ultrasonically processing for 30-60 minutes to obtain a uniform dispersion, coating the dispersion on a glassy carbon electrode. USE - Preparation of enzyme catalyzed three-dimensional porous graphene-carbon nanotube electrode. ADVANTAGE - The prepared electrode has good electroconductivity and enhances electron transport rate. The electrode structure provides more attachment sites for glucose oxidized enzymes. DETAILED DESCRIPTION - Preparation of enzyme catalyzed three-dimensional porous graphene-carbon nanotube electrode involves mixing graphene oxide solution and a carbon nanotube, stirring for 1-2 hours, placing the mixed solution in a reactor and reacting to 160-180 degrees C for 10-12 hours to obtain cylindrical three-dimensional graphene - carbon nanotube composite hydrogel, and freeze-drying to obtain powdery three-dimensional porous composite material, immersing the composite material in N,N-dimethylformamide and ultrasonically processing for 30-60 minutes to obtain a uniform dispersion, coating the dispersion on a glassy carbon electrode.