• 专利标题:   Preparing foamed graphene from antibiotic residue for preparing negative electrode active material for alkali metal ion battery, by performing solvothermal pretreatment, solid-liquid separating and two-stage gradient heat treatment.
  • 专利号:   CN112174119-A, CN112174119-B
  • 发明人:   TANG J, ZHOU X, GUO L, YANG J, WANG H, DING J, WANG J
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   C01B032/184, H01M010/0525, H01M004/587
  • 专利详细信息:   CN112174119-A 05 Jan 2021 C01B-032/184 202111 Pages: 16 Chinese
  • 申请详细信息:   CN112174119-A CN10885412 28 Aug 2020
  • 优先权号:   CN10885412

▎ 摘  要

NOVELTY - Method for preparing foamed graphene from antibiotic residue involves (i) performing solvothermal pretreatment on the solution containing antibiotic bacterium residue, alkali (A), and alcohol, and solid-liquid separation to obtain a pretreatment product, (ii) mixing the pretreatment product and alkali (B) and subjecting it to a two-stage gradient heat treatment to obtain the foamed graphene, where the two-stage gradient heat treatment process comprises the first stage heat treatment and second stage heat treatment, and the temperature of the first stage heat treatment is 300-500 degrees C, and the temperature of the second stage heat treatment is 600-1050 degrees C. USE - Method for preparing foamed graphene from antibiotic residue used for preparing negative electrode active material for alkali metal ion battery (all claimed), and in hazardous solid waste recovery. ADVANTAGE - The method realizes the high-value recycling and utilization of medical waste antibiotic bacteria residue, is environmentally-friendly, economical, and suitable for large-scale production and ensures short preparation process, excellent conductivity, high capacity and excellent cycle stability.