• 专利标题:   Preparation of loaded titania/MIL-53(Al) graphene oxide composite material used for adsorbing organic substance in sewage, by dissolving graphene oxide and aluminum nitrate nonahydrate and terephthalic acid into dimethylformamide solution.
  • 专利号:   CN112206746-A
  • 发明人:   CHENG L, WANG S
  • 专利权人:   CHENG L
  • 国际专利分类:   B01J020/20, B01J020/22, B01J020/30, C02F001/28, C02F001/30, C02F001/72, C02F101/30
  • 专利详细信息:   CN112206746-A 12 Jan 2021 B01J-020/22 202120 Pages: 7 Chinese
  • 申请详细信息:   CN112206746-A CN11122843 20 Oct 2020
  • 优先权号:   CN11122843

▎ 摘  要

NOVELTY - A loaded titania/MIL-53(Al) graphene oxide composite material is prepared by adding graphene oxide into dimethylformamide solution, ultrasonically processing to completely disperse, adding 0.005-0.015 mol aluminum nitrate nonahydrate and 0.005-0.015 mol terephthalic acid into dimethylformamide solution, stirring to completely dissolve, mixing two solutions, stirring for 1 hour, transferring into PTFE reaction kettle, hydrothermally reacting, cooling, centrifuging mixed solution at rate of 8000 revolutions/minute (rpm), washing using deionized water, vacuum drying, adding tetrabutyl titanate into anhydrous ethanol, vigorously stirring for 1 hour, dropping deionized water, continuously stirring and adding vacuum dried product, stirring for 1 hour, filtering and drying, putting in muffle furnace, and calcining at high temperature. USE - The method is used for preparing loaded titania/MIL-53(Al) graphene oxide composite material for adsorbing organic substance in sewage (claimed). ADVANTAGE - The product has excellent adsorption performance and stability.